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There are two major transitions in the relationship of shrinkage and additive concentration that can be explained by the sample morphology.
In a nanowire, nanoribbon, or nanosphere sample of Mn-doped ZnS nanostructures, the non-exponential decay behavior is influenced by the nanostructure geometry and can therefore be tuned by the sample morphology.
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The sample morphology was investigated by a transmission electron microscopy (TEM, JEM-2100F).
The sample morphology was evaluated by scanning electron microscopy (SEM, JEOL JSM-5900).
Further, the sample morphology was investigated by SEM (Figures 4 and 5).
The sample morphology was examined by field-emission scanning electron microscopy (FESEM) with a Hitachi S-4800 microscope.
The sample morphology is dominated by fibers that are aligned in a V-shaped, herringbone fashion.
The sample morphology has been characterized by scanning electron microscopy and transmission electron microscopy.
However, the sample morphology is clearly influenced by the amount of ionic liquid and in particular with its increase, the resulting particle morphology changes from octahedrons to spheres with porous surface.
The sample morphologies were examined by field emission scanning electron microscopy (FESEM) with a Hitachi S-4800 microscope (Dallas, TX, USA).
Observation of the samples' morphology by transmission electron microscopy (TEM) confirmed the results of X-ray diffraction methods.
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