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Elevated counts seen at ~6o 2θ are caused by the sample holder.
The effluent from macroporous resin column was first diluted and mixed with a derivatization reagent on-line, and the mixture was then directly transferred into the ionization region of DART-MS by the sample holder.
Thereafter, disks, 3 mm in diameter, were cut out from the obtained foil (the diameter was specified by the sample holder for the microscope), and a final thinning was done in the same solution.
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Tilt pair images were recorded by turning the sample holder around the tilt axis by 0° and 10°.
The Israeli team gets around these limits by sealing the sample holder with a thin polymer membrane -- covering the plate, as it were, with plastic wrap.
Mechanical stability was ensured by fixing the sample holder with plastic wrap inside the coil, which had also a damping effect on the sample holder.
Complex multilayers were produced by rotation of the sample holder and by controlling deposition conditions.
Uncertainties can also be caused by misalignment of the sample holder with respect to the measurement system of three interferometers.
In the middle panel, subfigure a shows temperature profiles measured by the thermocouple on the sample holder (green) and by an IR camera on the sample (purple).
The relative humidity was controlled by the temperature at the sample holder and steam generator.
The steam temperature was measured with a thermocouple at the outlet of the steam generating vessel, which was covered by heat insulating materials, and the sample holder temperature was monitored by two thermocouples installed close to the central part of the frictional surfaces (Fig. 2).
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