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Each formulation induces different degree of geopolymerization reaction as reflected by the phase composition where the amorphous phase is predominant.
These diffusion processes are greatly influenced by the phase composition of the coatings, especially by the presence of alpha-alumina.
The resulting photo electrochemical properties are to a large extent determined by the phase composition of the nanotubes (and not by the carbon content).
Samples were characterized by the phase composition of specimens using X-ray diffraction (XRD Siemens D-5000), with a Bragg − Brentano geometry and Cu − Kα radiation (λ = 1.5418 Å) using the following scan: step size = 0.02°, t = 5 s, 5° ≤ 2θ ≤ 70°.
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In our work, ultrafine lamellar eutectic structure was implemented by controlling the phase composition of eutectic reaction, and consequently by regulating the structure of eutectic reaction-induced liquid phase through varying component number.
We found that abrasive wear of the tool steel surface could be decreased by adapting the phase composition in the Al-base coating.
Finally, the phase composition (by XRD), microstructure (by SEM), mechanical characteristics, and the porosity of sintered samples were assessed.
The phase composition obtained by XRD was confirmed by a Raman microanalysis.
The phase composition is determined by XRD utilizing an equipment by Philips operated at 40 KV and 40 mA using Cu Kα radiation.
The coatings were investigated by X-ray diffraction to evaluate the phase composition, scanning electron microscopy and optical microscopy to calculate the surface density of macroparticles of the coating and their dimensions.
The chemical composition has been measured by electron energy loss spectroscopy, and the phase composition changes gradually from pure C to pure TiC or TiN through nanocomposite structures with variable phase contents.
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