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Therefore, the bulk viscosity of the sample is represented by the loss modulus [ 14].
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The storage modulus of high-generation dendrimer melts by far exceeds the loss modulus, furthermore, its value increases with temperature.
The amorphous phase contains a relatively homogeneous mixture of segments of both components indicated by the relatively uniform shape of the loss modulus peaks from dymamic-mechanical measurements for all investigated copolymers and blends.
The loss modulus curves were obtained by DMTA at frequency ω = 1 Hz.
A quantitative analysis of the β relaxation phenomena was performed by considering the loss compliance J″ instead of the loss modulus E″.
From, the traditional storage modulus G′ and the loss modulus G″ can be calculated by the incorporation of a geometric factor derived from finite element calculations [ 243, 258].
The visible viscosity differences were further quantified by dynamic rheological measurements of the storage modulus (G′) and the loss modulus (G″) as a function of frequency.
The method requires the measurement of the storage modulus (G′) and the loss modulus (G″) at a certain frequency (w) by oscillating viscosity measurements.
The loss modulus, G″, was smaller than the storage modulus at LVR, indicating a solid-like response, where most of the stress in the system is supported by the solid colloidal network structure.
Its real part is known as the storage modulus G ′ and the imaginary part is the loss modulus, G ′′.
At the glass transition, the storage modulus decreases dramatically and the loss modulus reaches a maximum (Agarwal et al. [2013]).
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