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The lifetime of the short-lived species (100 ns, 1560 cm–1) was reduced by purging the solution with oxygen.
The reaction was stirred at room temperature in the dark for 4 h, after which residual bromine was removed by purging the solution with nitrogen gas for 1 h.
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For all other experiments, anoxic conditions were established by purging the solutions permanently with Argon (Ar).
Unreacted TMA and by-products are removed by purging the chamber with HP Ar.
The performance can be recovered by purging the impurities from the anode channel.
We created anoxia by purging the headspaces of the bottles with nitrogen gas for two minutes.
This overall detection limit incorporates the error in measurement that arises from purging the initial solution into the KMnO4 solution, reducing the KMnO4 solution, diluting this reduced solution, and measuring the Hg concentration via CVAFS.
This was performed by firstly purging the system (xanthan solution with palm oil) with nitrogen gas until the dissolved oxygen fell to zero.
After purging the flask with H2, the solution was stirred overnight under light H2-pressure (balloon).
Sodium bisulfide solutions were prepared by purging dilute oxygen-free sodium hydroxide solution with high-purity 1% (v/v) hydrogen sulfide gas.
Argon gas was used to create anaerobic conditions by purging it into the medium.
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