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The surface morphologies by a systematic annealing process are shown with 2 nm thickness in Figure 1c and 9 nm thicknesses in Figure 1d.
Further confirmation of viscosity-and-shear-induced strain stored in the as-synthesized PEKs was provided by a systematic annealing study with differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD) analysis and Fourier-transform infrared spectroscopy (FT-IR).
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For a systematic annealing, a computer-operated recipe was run and the ramping-up rate was at 2.3°C/s under 1 × 10−4 Torr.
After a systematic annealing process, the resulting Au droplets are shown with the 3-nm deposition in Figure 1c and 6-nm DA in Figure 1d.
Figure 1d i show the evolution of PdAuAg nanostructures from the Pd/Au/Ag tri-metallic layers as shown in Fig. 1a by the systematic annealing between 400 and 900 °C for 450 s.
Figure 9 shows the Au droplet evolution as a function of the DA along with the systematic annealing at 550°C on GaAs (411 B, (711 B, (811 B, and (911 B, respectively.
Process parameters were optimized by conducting a systematic investigation.
In this work, we demonstrate various sizes and configurations of palladium (Pd) nanostructures on Si (111) by the systematic thermal annealing with the variation of Pd thickness and annealing temperature.
The hole mobility results of as-grown samples do not show a systematic behavior, while annealed samples do, depending on N concentration.
A systematic MDSC study of annealed samples revealed a wide spectrum of glass transition onsets, which show a strong dependence on the annealing conditions.
This is represented by a combination of steepest descent performed at the beginning and followed up by a simulated annealing.
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