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Raman spectroscopy revealed two broad peaks at 1386 cm− 1 and 1573 cm− 1 corresponding to the D and G peaks respectively.
In case of PFCzOxd-alt-PCz and PFCzCzPCz-co-PFOxdOxdPCz, the EL spectra of the polymers showed two distinct peaks comprising the maximum at 427 nm, which corresponds to the EL spectra of the conjugated backbone, and additional broad peaks at around 540 and 530 nm, respectively.
A doublet band of two broad peaks at 2166 and 2112 cm−1 is assigned to geminal CO on Rh surface oxide (or hydroxide) produced by the electrochemical modification process, and a doublet band of two peaks near 2103 and 2033 cm−1 is ascribed to geminal CO on surface clusters of Rh formed by reduction of Rh surface oxide.
Broad peaks at 1.41-1.77 ppm represent the CH2 groups' hydrogen.
The pattern was structureless, except for broad peaks at ca. 30° and ca. 45°.
The broad peaks at 619.2 and 534.2 represented C H bending.
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The spectra exhibit a sharp peak at ~−240 mV for 21-AGNR, a broad peak at ~−400 mV for 14-AGNR and a broader peak at ~−800 mV for 7-AGNR, as marked by green arrows, respectively.
A broad peak at 596 nm was observed for catalyst free growth of CdSe SPNR.
WXRD studies reveal that polythiophene shows a broad peak at 2θ value 18.23°.
The corresponding time-binned single-molecule histogram shows a narrow peak centred on ~ 1.0 and a broad peak at ~ 0.70 (Fig. 4b, bottom right).
For 7-AGNR, dI/dV spectra exhibit a broad peak at ~−850 mV at the edges and is almost featureless in the centre, as shown in Fig. 5a.
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