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In the preparation of nanocomposites via solution blending under vigorous stirring, two commercial organoclays (Southern Clay Products) were employed: one (Cloisite 30B) treated with a surfactant (MT2EtOH) having hydroxyl groups, and the other (Cloisite 20A) treated with a nonpolar surfactant (2M2HT) having hydrogenated tallow.
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The resulting solution was added into 33 ml of the as-prepared GO suspension under vigorous stirring at ambient temperature.
The mixture was then added dropwise into the chilled GO aqueous solution under vigorous stirring.
Binary blends of polystyrene (PS) and polyisoprene (PI) were prepared by rapidly precipitating a homogeneous solution, consisting of PS, PI and toluene, into methanol under vigorous agitation.
Under vigorous stirring methanol was added to eliminate the impurities.
The mixture was left under vigorous stirring for 2 h.
under vigorous stirring until a transparent solution was obtained.
TEOS was added to TPAOH solution under vigorous stirring.
On the other hand, fibers and bundles of threads resulted under vigorous and slow stirring conditions, respectively.
The whole mixture was heated to 85 °C under vigorous stirring until the solution became clear.
The resulting mixture was maintained at room temperature under vigorous stirring condition for 2 h.
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