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Collecting dates of the biological samples were recorded; whenever this information was not available, we included the year of the reference as proxy and indicated this in the observation.
H NMR spectra of all the biological samples were recorded at 298 K on a Bruker Avance III 600 MHz spectrometer (operating at 600.08 MHz for H) equipped with a Bruker inverse cryogenic probe (Bruker Biospin).
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Another recently developed targeting mass spectrometry (MS) approach is based on a data-independent acquisition (DIA) mass spectrometric method – SWATH MS. In contrast to SRM, in SWATH MS feature sets for all analytes detectable in a biological sample are recorded [13], which are then used to identify and quantify the respective analyte using a targeted data analysis strategy [13,14].
Some samples were recorded during the ceremonies.
Information from samples was recorded in questionnaires.
One hundred thousand events per sample were recorded.
The biological context of each sample was recorded and manually verified based on the sample descriptions in GEO (see Supplementary Method 1.1 and Supplementary Fig. S1).
The location where the sample was recorded.
Time of sampling was recorded.
The exact time of sampling was recorded.
Biological samples were processed at the U.S. Naval Medical Research Center Detachment in Lima, Peru.
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