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The experimental data reveal a strong correlation between the diffraction patterns and angular distributions of the scattering intensity.
Ordered hexagonal pore array structure of SBA-15 with Pd incorporated is preserved since no significant change between the diffraction patterns which indexed as (100), (110) and (200) for Pd/SBA-15 and SBA-15 materials (Figure 1).
Interestingly, high quality XRD patterns could be obtained by the μ-XRD approach, which allowed distinguishing between the diffraction patterns of zeolite Y, clay and boehmite.
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The X-ray diffraction investigations were obtained using a Bruker D8 Advance diffractometer, with nickel filtered Cu K (λ = 1.5418 Å) radiation and the diffraction patterns were recorded between 20° and 70° in the 2θ range with a step of 0.02° and 34 s measuring time per step.
A scan rate of 10 °C/min was used to record the diffraction patterns in 2θ range between 10 and 60 °C.
Furthermore, the features of the diffraction patterns are consistent with the presence of orientational correlations between adsorbed molecules.
The diffraction patterns are similar, as expected.
The X'Pert HighScore program was used to analyse the diffraction patterns and perform Rietveld refinements.
The analytical method that measures the diffraction patterns for the purpose of determining structure is termed X-ray diffraction analysis.
To construct difference diffraction patterns, it was necessary first to equalize the rotation and centering of the diffraction patterns by least-squares minimization of differences in the intensity of the 200 reflection between quadrants, using the Solver function in Microsoft Excel.
No other phases were identified in the diffraction patterns.
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