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The relationship between load and sample pressure was calibrated at 1600 °C using the following phase transformations: quartz coesite at 3.7 GPa (Kanzaki 1990); coesite stishovite at 10.26 GPa (Zhang et al. 1996); Mg2SiO4 at 15.2 GPa (Katsura et al. 2004).
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The viscosity of the system can be determined as a function of temperature and density from the sintering rate differences measured between loaded and unloaded samples.
The corresponding analysis indicates that the thermal activation model offers a good prediction for the variation of failure strain with respect to applied strain rate for failure mode I; the coupled evolution of atomic motions and potential landscapes governs the failure mode II; and the failure mode III is a result of the rapid separation between loading and deformation parts of the sample.
The sample size assignment to determined strata is done by considering the compatibility between load research objectives and sampling design and preparing the way to use the data and information provided by previous load research studies.
The relationship between peak area and sample loading was established at low sample loading, and found to be linear over an order of magnitude for both wet and dry modes with r2-values > 0.99.
Manual titrations require constant user intervention to wash cuvettes, load and thermostat samples between measurements.
Both age and time between disease onset and sampling were adjusted for in our calculations confirming the association between bacterial load and disease severity.
The relationship between the critical load and the strength of the glass sample was established.
Between each loading and reduction step the samples were thoroughly rinsed in ultrapure water.
σ f is calculated by the ratio between the maximum load and the initial cross section of the sample.
The degree of hydration varied considerably in PBS at pH 6.8 between the drug loaded and drug-free samples as depicted in Figure 6.
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