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The gap between electrodes was set by teflon fabric with 0.16 mm.
Distance between electrodes was set at 8 cm, and the pressure in the chamber after introducing nitrogen was 8 × 10-2 Torr.
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The spacing between the electrodes was set to 0.75 mm to adjust the minimum current density.
The surface area of each electrode was 678 mm2, and the spacing between two electrodes was set to be 0.8 mm.
The distance between two electrodes was set to 10, 15 and 20 cm and fibers were made accordingly.
The distance between the two electrodes was set to roughly zero as verified by measuring the resistance across the gap with a multimeter.
The interdistance between the working and counter electrodes was set at 1 cm.
At the initial stage, the gap between the two electrodes is set to a few angstroms (10−5 G0 < G < 10−4 G0) employing the MCBJ set-up.
The initial potential at the electrode was set as 1.582 V vs. RHE.
The working electrode was set at +400 mV against a silver/silver-chloride reference electrode.
The second electrode was set 250 mV for quantification.
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