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Water and Tris buffer showed the best extraction efficiency of all extractants used; however, the extraction efficiency was still less than 23%.
Experimental results indicated that the proposed MAE HS-SPME technique attained the best extraction efficiency of 106% recovery under the optiMAE HS-SPMEtechniquee. irrattained of exthection solution (10% aqueous ethylene glycol) at pH 5.0 with medium microwave power for 10 min. Desorption at 220 °C for 3 min offered the best dextractionefficiency
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The best extraction efficiencies of 78.6 and 73.7% were obtained for 1 mg L−1 citrate-stabilized Ag and TiO2 NPs, respectively, with 0.5 mM of 11-mercaptoundecanoic acid, 1.5 mM of octadecylamine, 1 mL of methanol, 150 μL of cyclohexane, 0.05 mM of tetra-n-octylammonium bromide, pH = 8.0, adsorption time of 2 h, sonication time of 3 min, and centrifugation time of 10 min.
Methanol, 80% methanol, 60% methanol and 40% methanol were used as extraction solvents (Additional file 1: Table S1), among which 80% methanol showed the best extraction efficiency for the six anthraquinone glycosides and was thus selected as the extraction solvent.
Some initial tests showed that the best extraction efficiency was obtained when using ultrasound instead of mechanical agitation, indicating that acoustic cavitation improved the extraction process.
Optimization of the variables affecting this method was carried out in order to achieve the best extraction efficiency.
Optimization of variables affecting the method was carried out in order to achieve the best extraction efficiency.
The affinity of the different derivatized compounds obtained towards five commercially available SPME coatings was evaluated, in order to achieve the best extraction efficiency.
The best extraction efficiencies were obtained at pressures near 14 MPa, for all the studied compounds.
The two fos-cholines had by far the best extraction efficiencies, close to 100%.
Besides, dry etching depth of PQC structure was approximately 95 nm which was optimized through various depth etching, (the data is not shown here) since this etching depth could attain the best performance of light extraction efficiency of our LED structure from our etching test experiments.
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