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The VFA showed an increasing tendency from the very beginning of sampling (Table 3).
With regard to individual VFAS, the acetate concentration rose rapidly from the very beginning of sampling.
The lactate-to-pyruvate ratio (La/Py ratio) reached its highest level at the beginning of sampling during anaesthesia with ratios varying from 38 to 75 and decreased thereafter.
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At the beginning of sample collection the written informed consent of patients was obtained for the use of their samples for diagnostic and scientific purposes.
At the beginning of sample analysis, an eight-point calibration curve was prepared covering the range from 0.05 to 50 ppb As.
Because the control status of subjects was designated at the beginning of sample selection for the nested case control, this study was analyzed as a case-cohort study [ 71].
From the various columns tested, only Phenyl HP was suited for CDH purification as with the other columns CDH binding was weak indicated by high c/c0 values right from the beginning of sample application (data not shown).
In animals that only had negative samples from the beginning of collection, sampling was terminated after 3 weeks PP.
Each sampling run required approximately 3 h, during which time meteorological conditions can change significantly; for this reason, stops 1 through 5, sampled at the beginning of each sampling run, were repeated at the end (as stops 21 25).
An important issue with sampling is the hardware state at the beginning of each sampling unit.
The surface concentrations obtained by DOSEC sampling are reported for each material at the beginning of the sampling campaign (September 2012) and at the end, 6 months later (March 2013).
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