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From the figure one can observe that it is a mixed nanocrystal region, because the diffraction pattern is a superposition of the patterns from two pieces of nanocrystals.
The sputtered CoO x on the stainless steel substrate indicated an amorphous nature because the diffraction pattern did not show any crystalline peaks from cobalt oxides, except the well-defined peaks from the stainless steel disc.
Because the diffraction pattern extended quite far in the vertical direction, the detector is not large enough to collect the full pattern in this direction.
Because the diffraction pattern surrounds a reciprocal lattice point is located far from the origin, the entire intensity distribution spans only a small angular range, which in most cases lies within a 1° sample rotation range.
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X-rays are used to produce the diffraction pattern because their wavelength λ is typically the same order of magnitude (1 100 angstroms) as the spacing d between planes in the crystal.
The diffraction pattern of triplite appears to be pseudo-hexagonal because the strongest reflections represent the substructure in the reciprocal lattice.
It can be seen that the diffraction pattern of the sample prepared at 300°C is indistinct because of the amorphous configuration.
By analyzing the diffraction pattern using software, scientists can make a map of the electron density in the crystal.
Subsequent analysis of the distribution of high intensity spots that makes up the diffraction pattern can then be used to reveal the underlying symmetry.
"I immediately recognised the diffraction pattern of wax as I encountered this material several times upon measuring paintings," Frederik Vanmeert, a PhD student at Antwerp, said.
The diffraction pattern of such a sequence closely resembles the fivefold symmetric patterns of Figure 3.
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