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Meanwhile, some mesopores with several nanometers in size can be clearly observed, which are scattering in the nanoflake array.
A Pt NP with a 32 nm diameter can be clearly observed, which coincides with our previous report about Ag tips [14].
Peaks located at around 400, 530, and 645 couldcould be clearly observed, which could be attributed to anatase TiO2 phase.
Before the set process, a broken region near the cathode as shown in Figure 4b (image b1) could be clearly observed, which limits the current flow, providing us a distinct evidence of HRS.
At this pH, a flat region from 700 mV to ∼0 V can be clearly observed, which indicates the potential range suitable for reduction of metals.
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In the through-plane visualization, N2 gas accumulation under the rib of anode and discharge to the channel was clearly observed, which are related with cell performance instability.
As illustrated in Fig. 4a, four characteristic peaks at 69.1, 104.1, 154.4, and 181.0 cm−1 respectively are clearly observed, which are consistent with the previous report [8, 22].
The interface between the MWCNTs and TiO2 is clearly observed, which confirms that the TiO2 nanoparticles were well attached to the surface of the MWCNTs.
A linear relationship is clearly observed, which further confirms that the dominating carrier transport process is the multistep tunneling mechanism [19, 21 23].
The fluctuations in J-V characteristic in both bias directions at 10 K are clearly observed, which reduces with increasing temperature and dies out at 40 K.
From the TEM images (Fig. 3c e), the porous nanosheets were clearly observed, which further confirms the formation of Zn0.8Mn0.2O porous nanostructures.
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com