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A predetermined amount of AgBr loaded TiO2 was dispersed in a 0.1% nafion in ethanol solution for 1 h in an ultrasonic bath to form a stable suspension.
Finally, the mixture was stirred at 60°C for 3 h in the water bath to form a transparent homogeneous mixture.
The inner water phase was mixed with the oil phase under stirring and then, the mixture was sonicated in an ice water bath to form a primary emulsion.
The solution was poured into defined amounts of aqueous solution containing 0.25% PVA and then probe sonicated at 80 W for 5 s and repeated three times in an ice-water bath to form a stable o/w emulsion.
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The mixture was then homogenized using a probe homogenizer (VIRTIS, Cyclone IQ, USA), at constant agitation speeds of 15000 rpm in an ice bath to form oil-in-water (O/W) emulsion.
The resulting primary emulsion was added to 5 ml distilled water containing PVA 1% (15000 MW, Sigma-Aldrich) and was sonicated for 60 sec at 100 W amplitude over an ice bath to form the double emulsion.
In the second set of experiments, dopes with varying shear histories were extruded into a non-solvent bath to form solid fibers.
Subsequently, the substrate with as-prepared Cu microcones was immersed into the plating bath to form Ni Co alloy nanocone coating on the surface of the Cu microcones.
The reactor system is then stirred at 480 to 500 rpm and cooled to a lower temperature of about 263.15 K using the Julabo® water bath to form semiclathrate hydrates.
There was a measurable depolarisation of the anode potential and also anode reaction of hydrogen and oxygen ions in the bath to form water vapour was confirmed by the water vapour condensate found at the electrolysis exit gas pipe.
The antisense-miRNA-spermidine complex was added dropwise to the stirred solution of PLGA- b-PEG polymer (10 mg) in dichloromethane (1 mL) containing 3%Span-80Span-80owed by sonication for 60 s at 40% amplitude in ice bath to form the first emulsion.
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