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The bath temperature was raised and maintained using a home-built system with an Omega CNPt series temperature controller (Stamford, CT).
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After evaporation of methanol under low pressure, the temperature was raised to 150°C using an oil bath to initiate the polymerization of the monomers.
The temperature was raised as required using the recirculating water bath and the pressure controlled using a hydraulic pump and measured using a pressure transducer.
When the resin concentration reached 70%, the temperature was raised to 20°C and the samples were placed in 3 consecutive baths of pure resin (lasting 1 h each) before polymerization at 60°C for 48 h.
Then sample temperature was raised to −160 °C.
Afterward, the temperature was raised to 70°CC.
The temperature was raised at 10 °C/min.
The temperature was raised to 800°C.
The temperature was raised to 37C.
The bath temperature was controlled via a PID temperature controller.
The bath temperature was maintained at 77 K.
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