The effects of solvent type on the morphology, thermal and mechanical properties of the nanocomposites were investigated by X-ray microtomography and diffraction, field emission scanning electron microscopy, analytical transmission electron microscopy based on electron loss spectroscopy imaging and dynamical mechanical analysis.
Further examination based on electron energy-loss spectroscopy (EELS) and energy-dispersive X-ray (EDX) analysis indicated that those particles are composed of ZnS clusters with the sizes of approximately 3 5 nm, which are produced as a by-product in the vulcanization.
A test based on electron spin resonance spectroscopy showed a reduced ability of HDL to stimulate endothelial NO production in patients with advanced CHD [13], [172].
Although a comprehensive membrane characterization based on electron paramagnetic resonance spectroscopy with spin labeling provided detailed information about overall membrane properties, it could not give spatial information about liposome-cell interaction.
Based on electron paramagnetic resonance (EPR) spectroscopy [3], [39] and X-ray-absorption near-edge structure (XANES) analyses [1], the dominant form of manganese in D. radiodurans cells is Mn2+, with no significant levels of Mn3+ detected.
Surface analysis based on Auger Electron Spectroscopy, Energy Dispersive Spectroscopy, and Scanning Electron Spectroscopy shows a significant reconstruction of the crystal surface after processing, namely, the appearance of numerous "volcano craters" and triangle-shaped defects with a typical size of 0.2 5.0 µm.
Based on Auger electron spectroscopy (AES), Fourier transform infrared absorption spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS), the film's chemical composition and microstructure is determined to be composed of a form of silicon carbide (SiC H) with organic moiety.
A series of shape evolutions of SrTiO3 crystallites varied gradually from the unfeatured conglomeration through eight-pod star-shaped particles to cubic crystals and have been recorded based on transmission electron spectroscopy (TEM) and scanning electron microscopy (SEM) observations.
In addition, both samples displayed an identical BET specific surface area of (1400±25) m g−1 and no differences were observable based on FTIR spectroscopy or electron microscopy.
