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They include traditional analytical techniques, such as atomic adsorption spectroscopy (AAS), atomic fluorescence spectroscopy (AFS), and atomic emission spectroscopy (AES).
The metal oxide content of the modified zeolites was determined by atomic adsorption spectroscopy (AAS) on a Perkin-Elmer AA 800 instrument.
After adsorption, the nanocomposite was taken from the solution and the residual Pb2+ concentration was measured using flame atomic adsorption spectroscopy.
Glass syringe fixed with nylon membrane filters having pore size of 0.45 µm was used to filter the solutions and finally analyzed by flame atomic adsorption spectroscopy.
The residual concentration of Pb2+ ions in aqueous media was analysed with the aid of Buck Scientifics 210 VGP flame atomic adsorption spectroscopy.
Experiments were done by treating aqueous standard solutions containing 0.1 mgL−1 of Fe(III), and subjected to flame atomic adsorption spectroscopy measurement.
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Standard solution of Zn2+ (1000 mg/L) for flame atomic adsorption spectrometry was obtained from Beijing NCS Analytical Instruments Co. Ltd.
The structure and composition of the catalyst materials were characterised by scanning electron microscopy, X-ray diffraction, X-ray photoelectron spectroscopy, atomic absorption spectroscopy and N2-adsorption analysis.
The analysis of batch adsorption of metal ions was carried out in 2 h and the concentration of each sample was measured by atomic absorption spectroscopy; first after 2 h, the adsorption percentage reached 84%, which may be due to the fact that the initial adsorbent sites were vacant and the solute concentration gradient was high.
X-ray adsorption spectroscopy.
The N doping decreases the hydrogen atomic adsorption energies.
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