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The size distribution of ADR-HSA NPs was tested by the dynamic laser light scattering instrument (DLLS, ALV/CGS-3, Germany) at the scattering angle of 30°.
It is important to show that the scattering from a stack of parallel planes remains in phase when Ω ≠ θB at the scattering angle 2θB.
The detector is located at the scattering angle of 90º.
The hydrodynamic diameter and size distribution were determined by ZetaSizer (Nano-ZS, Malvern Instruments, Worcestershire, UK) equipped with a HeeNe laser (633 nm) at the scattering angle 173°.
The hydrodynamic diameter and size distribution of micelles were studied by dynamic light scattering (DLS, ALV/CGS-3, Germany) instrument by dispersing the micelles (1 mg/mL) in Milli-Q water at the scattering angle of 90°.
Measurements were made at the scattering angle θ=173° ("backscattering detection") at 25 °C.
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The scattering spectra are not identical and the most probably reason for this is that the scattering angle at each position is not exactly the same, leading to a nonuniform spectral pattern even in this relatively small FoV (5 x 5 mm).
Angles in angle gathers refer to the scattering angle at the reflector and provide a natural access to analyzing migration velocity and amplitudes.
The scattering intensity I in the range of momentum transfer 0.01 < s < 0.45 Å-1 was recorded (s = 4πsinθ/λ, where λ = 1.5 Å is the X-ray wavelength and 2θ is the scattering angle) at a sample-detector distance of 2.7 m. Radiation damage, monitored by repetitive 15 s exposures, was negligible.
This change in the material causes a shift in the scattering angle (2θ) at a Bragg reflection (e.g., 002) and is one method by which to achieve imaging contrast (see below).
The scattering vector Q is defined as with the scattering angle δ and the wavelength λ.
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