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Statistical analysis of the pixel intensity variation offers the ability to distinguish appearance of crystals in the bulk solution and on the crystalliser walls.
The calcined fish bones exhibited an appearance of rod-like with micrometric size as shown in Figure 1. Figure 1 SEM photograph of fish bones used as target showing the size and appearance of crystals.
In his great work Urinary Deposits, Bird devotes much space to the identification of chemicals in urine by microscopic examination of the appearance of crystals in it.
He shows how the appearance of crystals of the same chemical can vary greatly under differing conditions, and especially how the appearance changes with disease.
This was confirmed by the kinetics of appearance of crystals within the nucleus of Ad-infected cells: intranuclear crystals were visible as early as 16 h pi, i.e. at early steps of the late phase of the virus life cycle (Fig. 3 I), indicating that crystal formation was contemporary to virion assembly.
If intranuclear penton crystals represented byproducts from viral capsid protein synthesis, one would expect that the appearance of crystals would be delayed in Ad-infected cell nucleus, compared to that of virus particles, and would constitute a very late event in the virus life cycle.
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Equatorial scattering maxima in the SAXS patterns for samples annealed at 75 °C were observed before the appearance of crystal reflections.
Microscopy studies have confirmed the presence of MSU crystals in the majority of those with ultrasonographic appearances of crystal deposition [ 26].
In particular, addition of gouty synovial fluid to supersaturated solutions of sodium urate resulted in a faster time to appearance of MSU crystals and a greater total weight of MSU crystals formed, compared to synovial fluid from healthy people and patients with RA or other crystal arthropathies [ 22, 27, 37, 38].
The crystals did not diffract with the home source and the appearance of the crystals was the same in both the control and the nanosphere drops.
Melting was detected by the appearance of quenched crystals of pyroxene, feldspar and glassy silica.
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