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In addition, this electrochemical oxidation was not observed in anhydrous atmosphere.
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The water molecules remained up to 80 °C, contributing to improve conductivity under an anhydrous N2 atmosphere.
Zhou and his co-workers also synthesized VN powder with a capacitance of 161 F g−1 at 30 mV s−1 by calcining V2O5 xerogel in a furnace under anhydrous NH3 atmosphere at 400 °C [24].
Polymer P1 (0.49 gram) and tetracyanoethylene (0.23 gram) were dissolved in 15 ml anhydrous DMF under nitrogen atmosphere.
It must be stored under a dry inert gas atmosphere or anhydrous mineral oil to prevent the formation of a surface layer of potassium superoxide.
All reactions involving moisture-sensitive reagents were conducted under argon atmosphere with anhydrous solvents and flame-dried glassware.
To a solution of 500 mg (2.1 mmol) of 7-hydroxyflavone in 10 mL of anhydrous pyridine under nitrogen atmosphere and cooling in an ice bath, 1.0 mL (5.9 mmol) of triflic anhydride was added.
Moreover, these catalysts are highly moisture-sensitive and hence require moisture-free solvent and reactants and anhydrous conditions, and also dry atmosphere for their handling [3].
A mixture of phosphorous oxychloride (0.3 ml) and 0.45 gram of polymer P1 were dissolved in 15 ml anhydrous DMF under the nitrogen atmosphere.
After heating the mixture of the Mo-HA precursor and anhydrous Na2SO4 in an argon atmosphere at a relatively high temperature, the Mo-HA precursor would be carbonized to form the intermediate of amorphous carbon, and then the intermediate would reduce anhydrous Na2SO4 to generate Na2S, further hydrolyzed to hydrogen sulfur.
Reactions were carried out under anhydrous conditions under a nitrogen atmosphere.
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