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The blood and urine samples shall be taken at the t0 and t2 sampling times.
The sampling site shall be the same as that of the organic regulated material or organic compound samples, and the samples shall be taken during the same time that the organic regulated material or organic compound samples are taken.
In very shallow waters where only a few of these would be pertinent, as a minimum, surface, mid-depth and bottom samples shall be taken, with samples at additional depths being added as indicated by local conditions.
Blood and tissue samples shall be taken at every visit (both initial and/or follow-up visits).
Samples shall be dry cleaned in a load that is 80% of the machine's capacity.
The minimum sampling time for each run shall be 1 hour in which either an integrated sample or a minimum of four grab samples shall be taken.
If grab sampling is used, then the samples shall be taken at approximately equal intervals in time, such as 15 minute intervals during the run.
These samples shall be preserved for subsequent analysis by or under the direct supervision of EPA laboratories in accordance with the approved plan of study.
For continuous unit operations and for a combination of both continuous and batch unit operations, the minimum sampling time for each run shall be 1 hour in which either an integrated sample or a minimum of four grab samples shall be taken.
The samples shall be analyzed at the Dr. Limbach Laboratory in Heidelberg.
Calcitonin ≥20 and <50 ng/l Calcitonin sampling shall be performed at intervals indicated in the study protocol with no further action unless levels rise to ≥50 ng/l.
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