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The precipitate was washed by distilled water and was dried in a vacuum oven at 120°C for 24 h.
Before the adhesion test, ultrasonication of the wires were done for 5 min in 2-propanol to remove adventitious macroscopic contaminations and were dried in a desiccator.
The nanoparticle and nanocomposite solutions were dropped on copper grids/glass slides and was dried in a dry air oven and was osmium coated for field emission scanning electron microscopy FE-SEM) (Fig. 3).
For TEM imaging, a small drop of the sample solution was dispersed onto a specific 3-mm carbon-coated copper grid and was dried in a desiccator at room temperature before TEM imagining.
Then, they were washed several times with deionized water on a filter paper with the pore size of 1 mm and were dried in a vacuum oven at 90 °C for 1 day.
The solid chars (hydrochars) obtained were washed gently with de-ionized water to remove any left over of the liquid phase of the reaction, and were dried in a conventional oven at 80 °C for 16 h.
Briefly, the excised gel slices were subjected to reduction and were dried in a vacuum centrifuge.
They had grain moisture levels in the usual range (i.e. 18 24 %) and were dried in a forced-air laboratory oven for 1 2 days down to a moisture level of about 10%%.
Seventy percent yield of the nanopowder was achieved and was dried in an oven at 65 °C, 1 h.
Greenish-black deposits remaining on the filter paper were washed by water and were dried in an electric oven at 60 °C for 12 h finally.
The biosorbent was filtered and was extensively washed with distilled water in order to get neutral product and was dried in an electric oven at (80 ± 2 °CC for 24 h.
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