Exact(30)
The presence of the known compounds in the active fractions was further confirmed by co-injection of the standard photosensitisers with fractions 2-16 in HPLC analytical runs.
Two rapid methods for highly selective detection and quantification of the two major glycoalkaloids in potatoes, α-chaconine and α-solanine, were compared for robustness in high-throughput operations for over 1000 analytical runs using potato tuber samples from field trials.
Costs are scaled by the projected number of analytical runs possible and include both energy source and control hardware.
Secondly, it enables a fast data processing using peak-picking and alignment software, which integrates m/z-signals, retention time and intensity features from several analytical runs [22].
In the HPFS, cases were assayed in four separate analytical runs (cases up to January 1996, February 1996-January 1998, February 1998-January 2000, and February 2000 January 2004) [21], [22].
Unless otherwise noted, all analytical runs used linear gradients of 30 100% buffer B in A (A: water containing 0.1% TFA, B: MeOH) over 70 min. CD Spectra were recorded on a Jasco J-815 Circular Dichroism Spectrometer.
Similar(30)
The analytical run was 4 min.
Each analytical run was prepared and assayed within a 28-h period.
The methods require only 200 μL of sample and allow a high throughput due to short analytical run (2 min).
The acceptance criterion for the ISR analytical run was 67%% (two-thirds of the total sample size) and should lie within 20%% difference (Viswanathan et al. 2007).
The experimental studies revealed that the first column was more suitable, since it produced well-resolved peaks with a very high sensitivity within a reasonable analytical run time.
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