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Samples were withdrawn periodically for analysis of reducing sugars (Miller 1959).
When GC MS or LC-ESI-MS/MS was employed for the analysis of carbohydrates, silylation, acetylation, methylation and trifluoroacetylation were the most popular derivatizing techniques [21, 22], but these single-step reactions were not suitable for the analysis of reducing sugar due to the variety of isomers that co-exist in aqueous solution [23, 24].
Samples were kept at -20°C prior to the analysis of reducing sugar concentration.
The supernatant was stored at -20°C prior to HPLC analysis of reducing sugar concentration.
We also thank Yi-Chin Wang and Jiun-Hau Lu for the analysis of reducing sugars.
Following digestion, the concentration of solubilised sugars was determined by the acid phenol method for analysis of reducing ends (Dubois et al., 1956).
Similar(53)
The experimental analysis of reduced scale flat slab models under punching, subject to in-plane forces is described and the results are compared with the Eurocode 2 (2004) [1] provisions, the FIP Recommendations for the Design of Post-tensioned Slabs and Foundation Rafts (1998) [2] and ACI 318-08 (2008) [3], to evaluate their validity.
284b Conversely, spectral analysis of reduced samples exposed to both SAM and tyrosine showed a significant decrease in the amount of [4Fe 4S]+ signal present, suggesting that tyrosine triggered the reduced [4Fe 4S]+ cluster to cleave SAM, generating the diamagnetic [4Fe 4S]2+ state.
This presents a different problem for the Fed than just delaying the taper by a meeting or two, this may require an entire recalibration of its analysis on reducing QE3.
A retrospective analysis of reduced-intensity conditioning in 110 consecutive recipients of HSCT from matched unrelated donors found that an rATG total dose of 6 mg/kg was associated with improved results compared with 8 mg/kg; the lower dose predicted improved relapse-free survival on multivariate analysis [ 235].
The results were obtained based on the analysis of total reducing sugars (TRS) with the DNS method.
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