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1H NMR studies of synthesized thiuram disulfides are performed on a Bruker DPX-400 spectrometer in CDCl3 with TMS as internal standard (chemical shift in δ) and CHN analysis is recorded on 2400 series II CHN analyzer Perkin Elmer.
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The AgNPs suspension was centrifuged at 10, 000 rpmin0 min and dried sample analysis was recorded on Perkin Elmer one IR spectrophotometer in the range from 450 to 3000 cm−1.
EDX analysis was recorded on Numerix DXP X10P.
ESIMS analysis were recorded on an API QSTAR Pulsar I spectrometer.
HPLC chromatograms for the amino acids analysis were recorded on a Waters model 600 Controller with Photodiode array detector 2487 (Waters, Milford, USA) and a 717 plus Waters automatic injector, with the software Millenium version 4.0.
The element analysis was recorded by energy-dispersive X-ray spectroscopy (EDS, AMETEK) attached on SEM.
Thermogravimetric and Differential thermal analysis measurements were recorded on a Perkin Elmer Pyris TGA/DTA under airflow with a heating rate 10 °C min−1.
The thermogravimetric analysis (TGA) was recorded on Mettler Toledo thermoanalyser under a nitrogen atmosphere at a heating rate of 10 °C/min from room temperature to 700 °C. Figure 1 represents the FTIR spectra of different compatibilizers (PE-g-MA, PP-g-MA and PS-g-MA) used in this study.
Fourier transform infrared spectroscopy FTIR analysis IR spectra were recorded on Shimadzu FT-IR, Prestige-21 spectrophotometer.
For off line analysis, regions of interest were recorded on video tapes using a S-VHS videocassette recorder AG-73500, Panasonic, Japan) at a rate of 50 frames/s and a digital camera (Kappa CF 8/1, Kappa Opto-electronics, Germany).
Circular disk and dendrite morphologies with great hexagonal symmetries were obtained, and the pattern formation mechanisms of ice crystals were defined on the basis of a precise analysis of videos that were recorded on the ISS and downlinked to us16,17,18.
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