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They were allowed to warm up naturally.
Samples were allowed to warm up to room temperature before analysis.
After the addition of Grignard reagent, the mixture was allowed to warm up to rt.
The mixture was allowed to warm to room temperature and stirred for 12 h.
The reaction mixture was then allowed to warm to room temperature and stirred.
The reaction mixture was allowed to warm to room temperature and left overnight.
Upon completion of the addition, the temperature of the reaction mixture was allowed to warm to room temperature.
The reaction mixture was slowly allowed to warm to 50°C and stirred vigorously for 24 h.
Stirring was continued for 1 h and the mixture was allowed to warm up to room temperature.
For each test, the block was removed from the mold and allowed to warm to room temperature for at least 4 h but less than 7 h.
After stirring for 30 min, the reaction temperature was allowed to warm to room temperature and continued stirring for additional 2 h.
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