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The SEM shows the agglomeration of nano-crystals.
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As shown, when the stirring time of reaction was increased, the intensity of the SPR peak also gradual increase until 24 h but after 48 h the SPR peak change to broad shape and intensity decreased, this phenomenon is related to the increased size and also agglomeration of silver nano-crystals [38].
This is due to the smaller size of nano-crystals present in the sample.
The deposited layer consisted of nano-crystals, as shown in the higher magnification image in Figure 1D.
The broad peaks formed by the nano alloy indicate the formation of nano crystals.
Formation of silicon nano-crystals takes place after RTA of these films.
b SEM image, ×30,500, demonstrating agglomeration of nano-hydroxyapatite particles filling the porous structure.
It is found that the agglomeration of nano materials is mostly lower than 4 μm in the mixtures.
Adding Cu nanoparticles into HA increased particle size and made coatings porous due to agglomeration of nano-sized particles.
This technique can effectively avoid the agglomeration of nano-particles in the coating matrix.
Due to high agglomeration of nano-TiO2 in cement media, their photocatalytic activity is significantly diminished.
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