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The resistive switching behavior was examined by applying the voltages as follows: 0 V → −10 V → 0 V → 10 V → 0 V with a sweeping rate of 0.1 V s−1.
The powder samples obtained were characterized for structural phase and nanosize formation using PANalytical X'Pert Pro X-ray diffractometer (The Netherlands) with Cu Kα (λ = 1.54 Å) in the range of 20° to 80° with a sweeping rate of 2°/min.
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The pear was placed in the middle of the vibration stage and excited by swept sine wave signals with a constant frequency sweeping rate and acceleration amplitude.
To find a better combination of test parameters, an L27 313) orthogonal test probing the frequency sweeping rate, acceleration amplitude, pear laying style, and their 2-way interactions was designed according to the results of the single-factor experiments.
The test parameter values required to obtain a better repeatability are as follows: frequency sweeping rate of 23.33 Hz/s with the linear frequency sweeping mode, acceleration amplitude of 1 g (g = 9.8 m/s2), and laying style that the pear is placed with its stem upward.
The sweep consistency is maintained as the sweeping rate increases, showing only some slight variations at 100 μs/step and some degradation at 20 μs/step.
The anodic and the cathodic polarization behaviour has been investigated under the various conditions by changing the potential region, sweeping rate, and concentration of an electrolyte.
The SS-OCT has a swept source OEM engine (AXSUN, λ 0 = 1060 n m, sweeping rate = 100 kHz, 3 dB axial resolution = 8 µm, scan range = 3.7 mm in air), a 2 x 2 coupler, a photodetector and a digitizer with a sampling rate of up to 500 MSPS with 12 bit resolution.
P3HexTh underwent electrochemical oxidation at about 0.4 V vs. Ag+/Ag in a THF solution, and the peak anode electric current, ipa, was proportional to the sweeping rate v; ipa=const×v1/2.
An acetylthiocholine concentration of 750 μM was used for the investigation of the sweeping rate effect.
Figure 7a displays their CV curves at the sweeping rate of 20 mV s 1.
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