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The second weight loss of 32.9% occurring at a starting temperature of 410°C to 500°C accompanied by a broad endothermic peak approximately at 450°C can be ascribed to the decomposition of the intermediate product, MgC2O4 to MgO.
The impact of the condensing temperature on pH was demonstrated using RTube at a starting temperature of -20 or -70°C [ 10].
The protocol utilized a starting temperature of 600 K. From 5 to 18 ps the temperature was decreased to 100 K.
Samples were run using full scan at a mass range of 50 to 500 m/z, with a 55 minute run time using a starting temperature of 70°C and a final temperature of 350°C.
A starting temperature of 35°C was held for 3 minutes and then ramped at 15°C/min to a temperature of 225°C and held for 1 minute, then continued at a ramped rate of 15°C/min to 300°C and held for 5 minutes.
For thermal stability, the molar ellipticity at λ = 222 nm was measured as the protein solutions were heated at a rate of 1 °C/min and used to determine the fraction of protein folded (assuming a completely folded protein population at a starting temperature of 10 °C).
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The results show that a minimum starting temperature of 152 °C and 63.8 W electric power are required to initiate the decrease of evaporation temperature.
Specifically, a lower starting temperature of 60 °C (vs. 70 °C) increased the response by over 400-fold for 1,4-BQ, (Fig. 2b) while still being able to acquire slower eluters like 1,4-B[c]PHEQ, 5,12-NAPQ, 7,12-B[a]ANCQ, and B[cd]PYRO in under 40 min (Fig. 3).
It was found that mechanical alloying has a significant influence on the starting temperature of the sintering process, microstructure, and distribution of elements.
For sesquiterpene analysis, a cool-on column inlet (starting temperature of 35 °C and track oven program after injection) was used to prevent thermo-rearrangements of terpenes in the injector.
When no amplified fragment was obtained with a primer pair, the touch-down starting temperature of annealing was decreased by 5°C until a successful amplification was achieved.
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