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The MRM quantitative analysis was performed on triple quadrupole mass spectrometer with optimized sensitivity and reproducibility.
The MRM sediment in May 2010 was excluded due to its exceptionally high PAH concentration.
The MRM transition monitored for DCU was m/z 225.4 to m/z 100.2.
The MRM sequence consisted of three periods executed sequentially to monitor different transition pairs using parameters optimised for each period.
The MRM studies were interpreted by two examiners.
The MRM approach demonstrates that 312 lipids could be monitored in 20 min [195].
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Moreover, the MRM-derived hydration values for mineralized zones were inversely correlated with mineral densities measured by XMT.
It is worth discussing the analytical performances of the MRM-based kinome profiling method.
In addition, we observed that the MRM-based method provided an excellent dynamic range for kinome quantification.
The development of the MRM-assay included the determination of major analytical parameters for DFC quantification in different matrices.
Characteristic product ions were at m/z 241.0, 227.0, and 210.0 completing the MRM-transitions for DFC quantification.
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