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The lowest degree of macro-particle contamination is observed at a duty cycle of about 40.5%.
The hardness of the coatings was the maximum (about 950 HV) at a duty cycle of 40%.
The intermittent discharge at a duty cycle of 20% required a process time of 20 s for the whole surface to experience the discharge.
Moderate ion bombardment at a duty cycle of 4.5% gives the highest (111)/(200) intensity ratio and the highest amount of TiN bonding.
High voltage pulses up to −10 kV at a duty cycle of 9% were used while the gas flow was varied between 20 and 50 sccm.
In the pulse-plating mode, samples with nearly uniform composition could be obtained at a duty cycle of 0.2 or smaller, and a continuous change in the composition profile could be seen as a function of the duty cycle above this value.
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