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Dichloromethane extract from leaves (1st collection) (9 g) was submitted to a chromatographic column (CC) fractionation on silica gel (332 g), eluted with gradients of hexane/ethyl acetate and ethyl acetate/methanol, yielding 99 fractions with 50 mL each.
On April 7th, 2009, the propolis samples considered as aged (M) (because they had remained in hives for at least 180 days) were collected (1st collection).
Each patient was sampled a 2nd time at 6 pm if the 1st collection was before noon, then at 6 am and pm on days 2-4, atd at 6 am on days 5-7.
All extracts showed activity against M. tuberculosis at least for one strain, except for the methanol extract of branches (1st collection) (Table 2).
Measurements done at the 1st collection of PL (T1) and a week after (T2) when possible.
We also collected another 10 donors (4 donors were identical from the 1st collection).
Similar(42)
39 collection.
Soulland's spring/summer 2014 collection.
Will Sienna Miller be wearing this outfit from her Twenty8Twelve collection next summer?
It's all in the Spa 7/52 collection.
'The Piano' was the source of my spring '94 collection".
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